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This paper reported the degradation of m-dihydroxybenzene aqueous solution with contact Glow Discharge Electrolysis.The rate of degradation in different conditions such as pH,H2O2,Fe2+,methanol,and other affecting factors were studied.The results showed that there is faster removal rate when the solution is in a relatively higher acidity;H2O2 can improve the efficiency rate.Fe2+can promote reaction,but radical elimination agent of methanol will decrease the rate of the reaction.