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High-voltage spinel LiNi0.5Mn1.5O4 (LNMO) is considered one of the most promising cathode material candidates for Li-ion rechargeable batteries (LIBs).The LNMO powders show a high voltage plateau at around 4.7 V, making its energy density (650 Wh/kg) 20% and 30% higher than that of conventionally used LiCoO2 and LiFePO4, respectively.